Journal article 1373 views 361 downloads
Solvent-free microwave-assisted synthesis of tenorite nanoparticle-decorated multi-walled carbon nanotubes
Journal of Materials Science & Technology, Volume: 35, Issue: 6, Pages: 1121 - 1127
Swansea University Authors:
Jennifer Rudd , Cathren Gowenlock
, Virginia Gomez
, Ewa Kazimierska, Enrico Andreoli
, Andrew Barron
-
PDF | Accepted Manuscript
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DOI (Published version): 10.1016/j.jmst.2019.01.002
Abstract
Copper-decorated carbon nanotubes (CNTs) have important applications as precursors for ultra-conductive copper wires. Tenorite-decorated CNTs (CuO-CNTs) are ideal candidate and are currently used in laborious processes. For this reason, we have developed a facile and scalable method for the synthesi...
Published in: | Journal of Materials Science & Technology |
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ISSN: | 10050302 |
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2019
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URI: | https://cronfa.swan.ac.uk/Record/cronfa48309 |
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2019-01-21T20:00:50Z |
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2019-03-11T14:00:19Z |
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2019-03-11T11:57:52.0238988 v2 48309 2019-01-21 Solvent-free microwave-assisted synthesis of tenorite nanoparticle-decorated multi-walled carbon nanotubes c2e4cf0f048a86b5ca2f331e6c566aff 0000-0002-5209-477X Jennifer Rudd Jennifer Rudd true false 3e999073c98799427c833bb5d331ef51 0000-0001-5774-5263 Cathren Gowenlock Cathren Gowenlock true false 2b0a7a13d79d306b3e0be7d30df54844 0000-0002-7846-9066 Virginia Gomez Virginia Gomez true false acd104d55246ee2d03420795510359e9 Ewa Kazimierska Ewa Kazimierska true false cbd843daab780bb55698a3daccd74df8 0000-0002-1207-2314 Enrico Andreoli Enrico Andreoli true false 92e452f20936d688d36f91c78574241d Andrew Barron Andrew Barron true false 2019-01-21 CBAE Copper-decorated carbon nanotubes (CNTs) have important applications as precursors for ultra-conductive copper wires. Tenorite-decorated CNTs (CuO-CNTs) are ideal candidate and are currently used in laborious processes. For this reason, we have developed a facile and scalable method for the synthesis of CuO-CNTs from copper acetate. It was found that the optimal loading of copper acetate onto the CNTs was 23.1 wt% and that three 1-minute microwave treatments were sufficient for the decomposition of copper acetate to copper oxide. The loading of copper oxide onto the nanotubes was confirmed using X-ray photoelectron spectroscopy, energy-dispersive X-ray spectroscopy and thermogravimetric analysis. The materials were characterised using X-ray diffraction and scanning electron microscopy. Journal Article Journal of Materials Science & Technology 35 6 1121 1127 10050302 microwave-assisted synthesis, multi-walled carbon nanotubes, tenorite, nanoparticle 30 6 2019 2019-06-30 10.1016/j.jmst.2019.01.002 COLLEGE NANME Management School COLLEGE CODE CBAE Swansea University 2019-03-11T11:57:52.0238988 2019-01-21T13:16:13.7509760 Faculty of Science and Engineering School of Engineering and Applied Sciences - Uncategorised Jennifer Rudd 0000-0002-5209-477X 1 Cathren Gowenlock 0000-0001-5774-5263 2 Virginia Gomez 0000-0002-7846-9066 3 Ewa Kazimierska 4 Abdullah M. Al-Enizi 5 Enrico Andreoli 0000-0002-1207-2314 6 Andrew Barron 7 0048309-21012019131924.pdf rudd2019.pdf 2019-01-21T13:19:24.1200000 Output 14626049 application/pdf Accepted Manuscript true 2020-01-11T00:00:00.0000000 true eng |
title |
Solvent-free microwave-assisted synthesis of tenorite nanoparticle-decorated multi-walled carbon nanotubes |
spellingShingle |
Solvent-free microwave-assisted synthesis of tenorite nanoparticle-decorated multi-walled carbon nanotubes Jennifer Rudd Cathren Gowenlock Virginia Gomez Ewa Kazimierska Enrico Andreoli Andrew Barron |
title_short |
Solvent-free microwave-assisted synthesis of tenorite nanoparticle-decorated multi-walled carbon nanotubes |
title_full |
Solvent-free microwave-assisted synthesis of tenorite nanoparticle-decorated multi-walled carbon nanotubes |
title_fullStr |
Solvent-free microwave-assisted synthesis of tenorite nanoparticle-decorated multi-walled carbon nanotubes |
title_full_unstemmed |
Solvent-free microwave-assisted synthesis of tenorite nanoparticle-decorated multi-walled carbon nanotubes |
title_sort |
Solvent-free microwave-assisted synthesis of tenorite nanoparticle-decorated multi-walled carbon nanotubes |
author_id_str_mv |
c2e4cf0f048a86b5ca2f331e6c566aff 3e999073c98799427c833bb5d331ef51 2b0a7a13d79d306b3e0be7d30df54844 acd104d55246ee2d03420795510359e9 cbd843daab780bb55698a3daccd74df8 92e452f20936d688d36f91c78574241d |
author_id_fullname_str_mv |
c2e4cf0f048a86b5ca2f331e6c566aff_***_Jennifer Rudd 3e999073c98799427c833bb5d331ef51_***_Cathren Gowenlock 2b0a7a13d79d306b3e0be7d30df54844_***_Virginia Gomez acd104d55246ee2d03420795510359e9_***_Ewa Kazimierska cbd843daab780bb55698a3daccd74df8_***_Enrico Andreoli 92e452f20936d688d36f91c78574241d_***_Andrew Barron |
author |
Jennifer Rudd Cathren Gowenlock Virginia Gomez Ewa Kazimierska Enrico Andreoli Andrew Barron |
author2 |
Jennifer Rudd Cathren Gowenlock Virginia Gomez Ewa Kazimierska Abdullah M. Al-Enizi Enrico Andreoli Andrew Barron |
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Journal of Materials Science & Technology |
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description |
Copper-decorated carbon nanotubes (CNTs) have important applications as precursors for ultra-conductive copper wires. Tenorite-decorated CNTs (CuO-CNTs) are ideal candidate and are currently used in laborious processes. For this reason, we have developed a facile and scalable method for the synthesis of CuO-CNTs from copper acetate. It was found that the optimal loading of copper acetate onto the CNTs was 23.1 wt% and that three 1-minute microwave treatments were sufficient for the decomposition of copper acetate to copper oxide. The loading of copper oxide onto the nanotubes was confirmed using X-ray photoelectron spectroscopy, energy-dispersive X-ray spectroscopy and thermogravimetric analysis. The materials were characterised using X-ray diffraction and scanning electron microscopy. |
published_date |
2019-06-30T10:04:39Z |
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1831904928235257856 |
score |
11.059359 |