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Micro-FTIR and Micro-Raman Studies of a Carbon Film Prepared from Furfuryl Alcohol Polymerization

S. Bertarione, F. Bonino, S. Jain, F. Cesano, M. Zanetti, D. Scarano, A. Zecchina, Sagar Jain

The Journal of Physical Chemistry B, Volume: 113, Issue: 31, Pages: 10571 - 10574

Swansea University Author: Sagar Jain

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DOI (Published version): 10.1021/jp9050534

Abstract

The synthesis of a carbon film by the acid-catalyzed polymerization and resinification of furfuryl alcohol with a diluted solution of HCl is studied by combining micro-FTIR and micro-Raman spectroscopies. The detailed study of the evolution of spectra as a function of dosage of furfuryl alcohol and...

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Published in: The Journal of Physical Chemistry B
ISSN: 1520-6106 1520-5207
Published: 2009
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URI: https://cronfa.swan.ac.uk/Record/cronfa32901
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last_indexed 2018-02-09T05:21:20Z
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spelling 2017-04-06T11:54:24.9045687 v2 32901 2017-04-02 Micro-FTIR and Micro-Raman Studies of a Carbon Film Prepared from Furfuryl Alcohol Polymerization 7073e179bb5b82db3e3efd3a8cd07139 Sagar Jain Sagar Jain true false 2017-04-02 The synthesis of a carbon film by the acid-catalyzed polymerization and resinification of furfuryl alcohol with a diluted solution of HCl is studied by combining micro-FTIR and micro-Raman spectroscopies. The detailed study of the evolution of spectra as a function of dosage of furfuryl alcohol and temperature shows that neutral and protonated species are formed at 80 °C, while upon gradually increasing the temperature up to 600 °C, the viscous polyfurfuryl alcohol resin is transformed into a carbon phase, containing a heterogeneous distribution of pores, with a size in the 100−2000 nm range, as shown by SEM and AFM analyses. Journal Article The Journal of Physical Chemistry B 113 31 10571 10574 1520-6106 1520-5207 31 12 2009 2009-12-31 10.1021/jp9050534 COLLEGE NANME COLLEGE CODE Swansea University 2017-04-06T11:54:24.9045687 2017-04-02T00:46:07.4854226 Faculty of Science and Engineering School of Engineering and Applied Sciences - Uncategorised S. Bertarione 1 F. Bonino 2 S. Jain 3 F. Cesano 4 M. Zanetti 5 D. Scarano 6 A. Zecchina 7 Sagar Jain 8
title Micro-FTIR and Micro-Raman Studies of a Carbon Film Prepared from Furfuryl Alcohol Polymerization
spellingShingle Micro-FTIR and Micro-Raman Studies of a Carbon Film Prepared from Furfuryl Alcohol Polymerization
Sagar Jain
title_short Micro-FTIR and Micro-Raman Studies of a Carbon Film Prepared from Furfuryl Alcohol Polymerization
title_full Micro-FTIR and Micro-Raman Studies of a Carbon Film Prepared from Furfuryl Alcohol Polymerization
title_fullStr Micro-FTIR and Micro-Raman Studies of a Carbon Film Prepared from Furfuryl Alcohol Polymerization
title_full_unstemmed Micro-FTIR and Micro-Raman Studies of a Carbon Film Prepared from Furfuryl Alcohol Polymerization
title_sort Micro-FTIR and Micro-Raman Studies of a Carbon Film Prepared from Furfuryl Alcohol Polymerization
author_id_str_mv 7073e179bb5b82db3e3efd3a8cd07139
author_id_fullname_str_mv 7073e179bb5b82db3e3efd3a8cd07139_***_Sagar Jain
author Sagar Jain
author2 S. Bertarione
F. Bonino
S. Jain
F. Cesano
M. Zanetti
D. Scarano
A. Zecchina
Sagar Jain
format Journal article
container_title The Journal of Physical Chemistry B
container_volume 113
container_issue 31
container_start_page 10571
publishDate 2009
institution Swansea University
issn 1520-6106
1520-5207
doi_str_mv 10.1021/jp9050534
college_str Faculty of Science and Engineering
hierarchytype
hierarchy_top_id facultyofscienceandengineering
hierarchy_top_title Faculty of Science and Engineering
hierarchy_parent_id facultyofscienceandengineering
hierarchy_parent_title Faculty of Science and Engineering
department_str School of Engineering and Applied Sciences - Uncategorised{{{_:::_}}}Faculty of Science and Engineering{{{_:::_}}}School of Engineering and Applied Sciences - Uncategorised
document_store_str 0
active_str 0
description The synthesis of a carbon film by the acid-catalyzed polymerization and resinification of furfuryl alcohol with a diluted solution of HCl is studied by combining micro-FTIR and micro-Raman spectroscopies. The detailed study of the evolution of spectra as a function of dosage of furfuryl alcohol and temperature shows that neutral and protonated species are formed at 80 °C, while upon gradually increasing the temperature up to 600 °C, the viscous polyfurfuryl alcohol resin is transformed into a carbon phase, containing a heterogeneous distribution of pores, with a size in the 100−2000 nm range, as shown by SEM and AFM analyses.
published_date 2009-12-31T04:00:20Z
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score 11.090009

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