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Micro-FTIR and Micro-Raman Studies of a Carbon Film Prepared from Furfuryl Alcohol Polymerization
The Journal of Physical Chemistry B, Volume: 113, Issue: 31, Pages: 10571 - 10574
Swansea University Author: Sagar Jain
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DOI (Published version): 10.1021/jp9050534
Abstract
The synthesis of a carbon film by the acid-catalyzed polymerization and resinification of furfuryl alcohol with a diluted solution of HCl is studied by combining micro-FTIR and micro-Raman spectroscopies. The detailed study of the evolution of spectra as a function of dosage of furfuryl alcohol and...
| Published in: | The Journal of Physical Chemistry B |
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| ISSN: | 1520-6106 1520-5207 |
| Published: |
2009
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| Online Access: |
Check full text
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| URI: | https://cronfa.swan.ac.uk/Record/cronfa32901 |
| Abstract: |
The synthesis of a carbon film by the acid-catalyzed polymerization and resinification of furfuryl alcohol with a diluted solution of HCl is studied by combining micro-FTIR and micro-Raman spectroscopies. The detailed study of the evolution of spectra as a function of dosage of furfuryl alcohol and temperature shows that neutral and protonated species are formed at 80 °C, while upon gradually increasing the temperature up to 600 °C, the viscous polyfurfuryl alcohol resin is transformed into a carbon phase, containing a heterogeneous distribution of pores, with a size in the 100−2000 nm range, as shown by SEM and AFM analyses. |
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| College: |
Faculty of Science and Engineering |
| Issue: |
31 |
| Start Page: |
10571 |
| End Page: |
10574 |