Journal article 866 views
In situ TEM studies of micron-sized all-solid-state fluoride ion batteries: Preparation, prospects, and challenges
,
Carine Rongeat,
Torsten Scherer,
Horst Hahn,
Maximilian Fichtner,
Christian Kübel
Microscopy Research and Technique, Volume: 79, Issue: 7, Pages: 615 - 624
Swansea University Author:
Anji Munnangi
Full text not available from this repository: check for access using links below.
DOI (Published version): 10.1002/jemt.22675
Abstract
Trustworthy preparation and contacting of micron‐sized batteries is an essential task to enable reliable in situ TEM studies during electrochemical biasing. Some of the challenges and solutions for the preparation of all‐solid‐state batteries for in situ TEM electrochemical studies are discussed usi...
| Published in: | Microscopy Research and Technique |
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| ISSN: | 1059-910X |
| Published: |
Wiley
2016
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| Online Access: |
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| URI: | https://cronfa.swan.ac.uk/Record/cronfa51559 |
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| Abstract: |
Trustworthy preparation and contacting of micron‐sized batteries is an essential task to enable reliable in situ TEM studies during electrochemical biasing. Some of the challenges and solutions for the preparation of all‐solid‐state batteries for in situ TEM electrochemical studies are discussed using an optimized focused ion beam (FIB) approach. In particular redeposition, resistivity, porosity of the electrodes/electrolyte and leakage current are addressed. Overcoming these challenges, an all‐solid‐state fluoride ion battery has been prepared as a model system for in situ TEM electrochemical biasing studies and first results on a Bi/La0.9Ba0.1F2.9 half‐cell are presented. |
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| College: |
Faculty of Science and Engineering |
| Issue: |
7 |
| Start Page: |
615 |
| End Page: |
624 |