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Efficient microwave assisted synthesis of metal–organic framework UiO-66: optimization and scale up

M. Taddei, P. Dau, S. Cohen, M. Ranocchiari, J. van Bokhoven,, F. Costantino, S. Sabatini, R. Vivani, Marco Taddei Orcid Logo

Dalton Trans., Volume: 44, Issue: 31, Pages: 14019 - 14026

Swansea University Author: Marco Taddei Orcid Logo

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DOI (Published version): 10.1039/c5dt01838b

Abstract

A highly efficient and scalable microwave assisted synthesis of zirconium-based metal–organic framework UiO-66 was developed. In order to identify the best conditions for optimizing the process, a wide range of parameters was investigated. The efficiency of the process was evaluated with the aid of...

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Published in: Dalton Trans.
ISSN: 1477-9226 1477-9234
Published: Royal Society of Chemistry (RSC) 2015
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URI: https://cronfa.swan.ac.uk/Record/cronfa32747
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first_indexed 2017-03-29T13:47:15Z
last_indexed 2018-02-09T05:21:00Z
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spelling 2017-04-03T11:29:16.0731389 v2 32747 2017-03-29 Efficient microwave assisted synthesis of metal–organic framework UiO-66: optimization and scale up 5cffd1038508554d8596dee8b4e51052 0000-0003-2805-6375 Marco Taddei Marco Taddei true false 2017-03-29 EEN A highly efficient and scalable microwave assisted synthesis of zirconium-based metal–organic framework UiO-66 was developed. In order to identify the best conditions for optimizing the process, a wide range of parameters was investigated. The efficiency of the process was evaluated with the aid of four quantitative indicators. The properties of the materials prepared by microwave irradiation were compared with those synthesized by conventional heating, and no significant effects on morphology, crystal size, or defects were found from the use of microwave assisted heating. Scale up was performed maintaining the high efficiency of the process. Journal Article Dalton Trans. 44 31 14019 14026 Royal Society of Chemistry (RSC) 1477-9226 1477-9234 7 7 2015 2015-07-07 10.1039/c5dt01838b COLLEGE NANME Engineering COLLEGE CODE EEN Swansea University 2017-04-03T11:29:16.0731389 2017-03-29T09:52:40.4021317 Faculty of Science and Engineering School of Engineering and Applied Sciences - Uncategorised M. Taddei 1 P. Dau 2 S. Cohen 3 M. Ranocchiari 4 J. van Bokhoven, 5 F. Costantino 6 S. Sabatini 7 R. Vivani 8 Marco Taddei 0000-0003-2805-6375 9
title Efficient microwave assisted synthesis of metal–organic framework UiO-66: optimization and scale up
spellingShingle Efficient microwave assisted synthesis of metal–organic framework UiO-66: optimization and scale up
Marco Taddei
title_short Efficient microwave assisted synthesis of metal–organic framework UiO-66: optimization and scale up
title_full Efficient microwave assisted synthesis of metal–organic framework UiO-66: optimization and scale up
title_fullStr Efficient microwave assisted synthesis of metal–organic framework UiO-66: optimization and scale up
title_full_unstemmed Efficient microwave assisted synthesis of metal–organic framework UiO-66: optimization and scale up
title_sort Efficient microwave assisted synthesis of metal–organic framework UiO-66: optimization and scale up
author_id_str_mv 5cffd1038508554d8596dee8b4e51052
author_id_fullname_str_mv 5cffd1038508554d8596dee8b4e51052_***_Marco Taddei
author Marco Taddei
author2 M. Taddei
P. Dau
S. Cohen
M. Ranocchiari
J. van Bokhoven,
F. Costantino
S. Sabatini
R. Vivani
Marco Taddei
format Journal article
container_title Dalton Trans.
container_volume 44
container_issue 31
container_start_page 14019
publishDate 2015
institution Swansea University
issn 1477-9226
1477-9234
doi_str_mv 10.1039/c5dt01838b
publisher Royal Society of Chemistry (RSC)
college_str Faculty of Science and Engineering
hierarchytype
hierarchy_top_id facultyofscienceandengineering
hierarchy_top_title Faculty of Science and Engineering
hierarchy_parent_id facultyofscienceandengineering
hierarchy_parent_title Faculty of Science and Engineering
department_str School of Engineering and Applied Sciences - Uncategorised{{{_:::_}}}Faculty of Science and Engineering{{{_:::_}}}School of Engineering and Applied Sciences - Uncategorised
document_store_str 0
active_str 0
description A highly efficient and scalable microwave assisted synthesis of zirconium-based metal–organic framework UiO-66 was developed. In order to identify the best conditions for optimizing the process, a wide range of parameters was investigated. The efficiency of the process was evaluated with the aid of four quantitative indicators. The properties of the materials prepared by microwave irradiation were compared with those synthesized by conventional heating, and no significant effects on morphology, crystal size, or defects were found from the use of microwave assisted heating. Scale up was performed maintaining the high efficiency of the process.
published_date 2015-07-07T03:40:14Z
_version_ 1763751823080947712
score 11.01753

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