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Aging of the reaction mixture as a tool to modulate the crystallite size of UiO-66 into the low nanometer range

Marco Taddei Orcid Logo, Kim Corinna Dümbgen, Jeroen Anton van Bokhoven, Marco Ranocchiari

Chemical Communications, Volume: 52, Issue: 38, Pages: 6411 - 6414

Swansea University Author: Marco Taddei Orcid Logo

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DOI (Published version): 10.1039/c6cc02517j

Abstract

Nanosized UiO-66 with an unprecedented crystallite size of 10 nm was synthesized by exploiting controlled aging of stock solutions of Zr4+ in N,N-dimethylformamide in the presence of variable amounts of water and acetic acid prior to the addition of the ligand. The yield of the synthesis is not affe...

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Published in: Chemical Communications
ISSN: 1359-7345 1364-548X
Published: Royal Society of Chemistry (RSC) 2016
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URI: https://cronfa.swan.ac.uk/Record/cronfa32744
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first_indexed 2017-03-29T13:47:15Z
last_indexed 2018-02-09T05:20:59Z
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spelling 2017-07-07T15:49:22.2797466 v2 32744 2017-03-29 Aging of the reaction mixture as a tool to modulate the crystallite size of UiO-66 into the low nanometer range 5cffd1038508554d8596dee8b4e51052 0000-0003-2805-6375 Marco Taddei Marco Taddei true false 2017-03-29 EEN Nanosized UiO-66 with an unprecedented crystallite size of 10 nm was synthesized by exploiting controlled aging of stock solutions of Zr4+ in N,N-dimethylformamide in the presence of variable amounts of water and acetic acid prior to the addition of the ligand. The yield of the synthesis is not affected, affording high conversion of the starting reagents into the product. Journal Article Chemical Communications 52 38 6411 6414 Royal Society of Chemistry (RSC) 1359-7345 1364-548X 11 4 2016 2016-04-11 10.1039/c6cc02517j COLLEGE NANME Engineering COLLEGE CODE EEN Swansea University 2017-07-07T15:49:22.2797466 2017-03-29T09:52:37.5629000 Faculty of Science and Engineering School of Engineering and Applied Sciences - Uncategorised Marco Taddei 0000-0003-2805-6375 1 Kim Corinna Dümbgen 2 Jeroen Anton van Bokhoven 3 Marco Ranocchiari 4
title Aging of the reaction mixture as a tool to modulate the crystallite size of UiO-66 into the low nanometer range
spellingShingle Aging of the reaction mixture as a tool to modulate the crystallite size of UiO-66 into the low nanometer range
Marco Taddei
title_short Aging of the reaction mixture as a tool to modulate the crystallite size of UiO-66 into the low nanometer range
title_full Aging of the reaction mixture as a tool to modulate the crystallite size of UiO-66 into the low nanometer range
title_fullStr Aging of the reaction mixture as a tool to modulate the crystallite size of UiO-66 into the low nanometer range
title_full_unstemmed Aging of the reaction mixture as a tool to modulate the crystallite size of UiO-66 into the low nanometer range
title_sort Aging of the reaction mixture as a tool to modulate the crystallite size of UiO-66 into the low nanometer range
author_id_str_mv 5cffd1038508554d8596dee8b4e51052
author_id_fullname_str_mv 5cffd1038508554d8596dee8b4e51052_***_Marco Taddei
author Marco Taddei
author2 Marco Taddei
Kim Corinna Dümbgen
Jeroen Anton van Bokhoven
Marco Ranocchiari
format Journal article
container_title Chemical Communications
container_volume 52
container_issue 38
container_start_page 6411
publishDate 2016
institution Swansea University
issn 1359-7345
1364-548X
doi_str_mv 10.1039/c6cc02517j
publisher Royal Society of Chemistry (RSC)
college_str Faculty of Science and Engineering
hierarchytype
hierarchy_top_id facultyofscienceandengineering
hierarchy_top_title Faculty of Science and Engineering
hierarchy_parent_id facultyofscienceandengineering
hierarchy_parent_title Faculty of Science and Engineering
department_str School of Engineering and Applied Sciences - Uncategorised{{{_:::_}}}Faculty of Science and Engineering{{{_:::_}}}School of Engineering and Applied Sciences - Uncategorised
document_store_str 0
active_str 0
description Nanosized UiO-66 with an unprecedented crystallite size of 10 nm was synthesized by exploiting controlled aging of stock solutions of Zr4+ in N,N-dimethylformamide in the presence of variable amounts of water and acetic acid prior to the addition of the ligand. The yield of the synthesis is not affected, affording high conversion of the starting reagents into the product.
published_date 2016-04-11T03:40:13Z
_version_ 1763751822712897536
score 11.013148

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